dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene

Base Information

Chemical Name:dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene
CAS No.:1321606-24-9
Molecular Formula:C₆₄H₅₂
Molecular Weight:821.117
Hs Code.:

Synonyms:dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene

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Chemical Property of dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene

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Technology Process of dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene

There total 3 articles about dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1321606-21-6
7-(cyclohex-1-en-1-yl)-12-phenyl-8,9,10,11-tetrahydrobenzo[k]fluoranthene

: 1321606-24-9
dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene

Guidance literature:: With methanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 - 5 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201100858

Reference yield:

: 98-80-6
phenylboronic acid

: 1321606-24-9
dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 5 h / 100 °C / Inert atmosphere; Sealed flask

2: methanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 - 5 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; methanesulfonic acid; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol; dichloromethane; toluene; 1: Suzuki coupling / 2: Scholl reaction;
DOI:10.1002/chem.201100858

Reference yield:

: 1321605-37-1
7-(cyclohex-1-en-1-yl)-12-iodo-8,9,10,11-cyclohenta[k]fluoranthene

: 1321606-24-9
dibenzo{[f,f]-4,7'-diphenyl-4',7-bis(cyclohex-1-en-1-yl)}diindeno[1,2,3-cd:1',2',3'-lm]perylene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 5 h / 100 °C / Inert atmosphere; Sealed flask

2: methanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 - 5 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; methanesulfonic acid; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol; dichloromethane; toluene; 1: Suzuki coupling / 2: Scholl reaction;
DOI:10.1002/chem.201100858