2'-(2,3-dihydroxy-3-methylbutyl)-4'-(hydroxymethyl)trifluoroacetanilide

Base Information

Chemical Name:2'-(2,3-dihydroxy-3-methylbutyl)-4'-(hydroxymethyl)trifluoroacetanilide
CAS No.:130074-96-3
Molecular Formula:C₁₄H₁₈F₃NO₄
Molecular Weight:321.296
Hs Code.:

Synonyms:2'-(2,3-dihydroxy-3-methylbutyl)-4'-(hydroxymethyl)trifluoroacetanilide

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Chemical Property of 2'-(2,3-dihydroxy-3-methylbutyl)-4'-(hydroxymethyl)trifluoroacetanilide

Chemical Property:

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Technology Process of 2'-(2,3-dihydroxy-3-methylbutyl)-4'-(hydroxymethyl)trifluoroacetanilide

There total 2 articles about 2'-(2,3-dihydroxy-3-methylbutyl)-4'-(hydroxymethyl)trifluoroacetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 130074-89-4
2'-(2,3-epoxy-3-methylbutyl)trifluoroacetanilide

: 130074-96-3
2'-(2,3-dihydroxy-3-methylbutyl)-4'-(hydroxymethyl)trifluoroacetanilide

Guidance literature:: With boron trifluoride diethyl etherate; In diethyl ether; for 0.0833333h;

Reference yield:

: 130074-91-8
2,2,2-trifluoro-N-<2-(3-methylbut-2-enyl)phenyl>acetamide

: 130074-96-3
2'-(2,3-dihydroxy-3-methylbutyl)-4'-(hydroxymethyl)trifluoroacetanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 3 h

2: 83 percent / boron trifluoride etherate / diethyl ether / 0.08 h

With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;