C₂₂H₁₇FN₄O

Base Information

Chemical Name:C₂₂H₁₇FN₄O
CAS No.:1620955-66-9
Molecular Formula:C₂₂H₁₇FN₄O
Molecular Weight:372.402
Hs Code.:

C<sub>22</sub>H<sub>17</sub>FN<sub>4</sub>O

Synonyms:C₂₂H₁₇FN₄O

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Chemical Property of C₂₂H₁₇FN₄O

Chemical Property:

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Technology Process of C₂₂H₁₇FN₄O

There total 4 articles about C₂₂H₁₇FN₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1620955-65-8
C₁₆H₁₃BrN₄O

: 1765-93-1
4-fluoroboronic acid

: 1620955-66-9
C₂₂H₁₇FN₄O

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,4-dioxane; methanol; water; at 90 ℃; for 5h; Inert atmosphere;

Reference yield:

: 1054478-77-1
2-(4-bromophenyl)-1,6-naphthyridine-4-carboxylic acid

: 1620955-66-9
C₂₂H₁₇FN₄O

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; diphenyl phosphoryl azide / 18 h / Reflux

2.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2.17 h / 0 - 20 °C / Inert atmosphere

3.2: 3 h / 0 - 100 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / water; 1,4-dioxane; methanol / 5 h / 90 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; sodium hydride; caesium carbonate; triethylamine; trifluoroacetic acid; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1620955-18-1
C₁₉H₁₈BrN₃O₂

: 1620955-66-9
C₂₂H₁₇FN₄O

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2.17 h / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 0 - 100 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / water; 1,4-dioxane; methanol / 5 h / 90 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; caesium carbonate; trifluoroacetic acid; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;