N-(t-Butoxycarbonyl)-2,3-bis-1H-pyrrole

Base Information

• Chemical Name: N-(t-Butoxycarbonyl)-2,3-bis-1H-pyrrole
• CAS No.: 82912-40-1
• Molecular Formula: C₁₁H₁₁F₆NO₂
• Molecular Weight: 303.204
• Mol file: 82912-40-1.mol

Synonyms:N-(t-Butoxycarbonyl)-2,3-bis-1H-pyrrole

Chemical Property of N-(t-Butoxycarbonyl)-2,3-bis-1H-pyrrole

Chemical Property:

Purity/Quality:

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Technology Process of N-(t-Butoxycarbonyl)-2,3-bis-1H-pyrrole

There total 1 articles about N-(t-Butoxycarbonyl)-2,3-bis-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

N-(t-Butoxycarbonyl)-2,3-bis-7-azabicyclo<2.2.1>hepta-2,5-diene (82912-39-8) → 3-(2,4,6-trimethyl-phenyl)-isoxazole (49748-48-3) + N-tert-butyloxycarbonyl-pyrrole (5176-27-2) + N-(t-Butoxycarbonyl)-2,3-bis-1H-pyrrole (82912-40-1) + 4,5-Bis-trifluoromethyl-3-(2,4,6-trimethyl-phenyl)-isoxazole

Guidance literature:

With mesitylenecarbonitrile oxide; In diethyl ether; at 30 ℃; for 24h;

DOI:10.1055/s-1982-29795

Reference yield: 80.0%

N-(t-Butoxycarbonyl)-2,3-bis-1H-pyrrole (82912-40-1) → 3,4-Bis-1H-pyrrole (82912-41-2)

Guidance literature:

at 160 ℃; for 0.5h;

DOI:10.1055/s-1982-29795

upstream raw materials:

N-(t-Butoxycarbonyl)-2,3-bis-7-azabicyclo<2.2.1>hepta-2,5-diene

Downstream raw materials:

3,4-Bis-1H-pyrrole