C₅₁H₅₅N₃O₁₀

Base Information

Chemical Name:C₅₁H₅₅N₃O₁₀
CAS No.:1330717-05-9
Molecular Formula:C₅₁H₅₅N₃O₁₀
Molecular Weight:870.012
Hs Code.:

C<sub>51</sub>H<sub>55</sub>N<sub>3</sub>O<sub>10</sub>

Synonyms:C₅₁H₅₅N₃O₁₀

Suppliers and Price of C₅₁H₅₅N₃O₁₀

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₁H₅₅N₃O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₁H₅₅N₃O₁₀

There total 9 articles about C₅₁H₅₅N₃O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1330717-01-5
C₃₇H₃₇N₃O₇

: 742101-64-0
2-[2-(1-bromo-vinyl)-3-methoxy-5-methyl-phenyl]-[1,3]dioxane

: 1330717-05-9
C₅₁H₅₅N₃O₁₀

Guidance literature:: 2-[2-(1-bromo-vinyl)-3-methoxy-5-methyl-phenyl]-[1,3]dioxane; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 0.166667h; Inert atmosphere;

C₃₇H₃₇N₃O₇; In diethyl ether; pentane; at -78 - -50 ℃; for 1.66667h; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.046

Reference yield:

: C₄₁H₄₉N₃O₈Si

: 1330717-05-9
C₅₁H₅₅N₃O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen fluoride; water / acetonitrile / 1.5 h / 0 °C

2.1: hydrogenchloride; water / 1,2-dimethoxyethane / 6 h / 40 °C

3.1: toluene-4-sulfonic acid / methanol / 18 h / 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 25 h / 20 °C

5.1: tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C / Inert atmosphere

5.2: 1.67 h / -78 - -50 °C / Inert atmosphere

With hydrogenchloride; hydrogen fluoride; water; tert.-butyl lithium; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; 1,2-dimethoxyethane; diethyl ether; dimethyl sulfoxide; acetonitrile; pentane;
DOI:10.1016/j.tet.2011.06.046

Reference yield:

: C₃₇H₃₇N₃O₇

: 1330717-05-9
C₅₁H₅₅N₃O₁₀

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; water / 1,2-dimethoxyethane / 6 h / 40 °C

2.1: toluene-4-sulfonic acid / methanol / 18 h / 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 25 h / 20 °C

4.1: tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C / Inert atmosphere

4.2: 1.67 h / -78 - -50 °C / Inert atmosphere

With hydrogenchloride; water; tert.-butyl lithium; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; 1,2-dimethoxyethane; diethyl ether; dimethyl sulfoxide; pentane;
DOI:10.1016/j.tet.2011.06.046