C₅₅H₇₈O₁₀SSi₂

Base Information

Chemical Name:C₅₅H₇₈O₁₀SSi₂
CAS No.:1592771-29-3
Molecular Formula:C₅₅H₇₈O₁₀SSi₂
Molecular Weight:987.455
Hs Code.:

C<sub>55</sub>H<sub>78</sub>O<sub>10</sub>SSi<sub>2</sub>

Synonyms:C₅₅H₇₈O₁₀SSi₂

Suppliers and Price of C₅₅H₇₈O₁₀SSi₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₅H₇₈O₁₀SSi₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₅H₇₈O₁₀SSi₂

There total 30 articles about C₅₅H₇₈O₁₀SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1592771-13-5
C₂₉H₄₂O₆SSi

: 1592770-91-6
C₂₇H₃₇F₃O₇SSi

: 1592771-29-3
C₅₅H₇₈O₁₀SSi₂

Guidance literature:: With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -100 ℃; for 0.666667h; Temperature; Inert atmosphere;
DOI:10.1021/ol500788c

Reference yield:

: methyl 3-O-benzyl-5-O-(p-toluenesulfonyl)-2-deoxy-D-ribofuranoside

: 1592771-29-3
C₅₅H₇₈O₁₀SSi₂

Guidance literature:: Multi-step reaction with 10 steps

1: lithium triethylborohydride / tetrahydrofuran / 6.25 h / 20 - 45 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 - 20 °C / Inert atmosphere

3: 4-methyl-morpholine / dichloromethane / 2 h / 20 °C / Inert atmosphere

4: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 24 h / 20 °C

5: samarium diiodide / acetonitrile; methanol / 1 h / -20 °C / Inert atmosphere

6: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

7: diisobutylaluminium hydride / dichloromethane; hexane / 0.75 h / -80 °C / Inert atmosphere

8: lithium chloride; triethylamine / acetonitrile / 5 h / 20 °C / Inert atmosphere

9: potassium tert-butylate; tert.-butylhydroperoxide / tetrahydrofuran / 16 h / -80 - -25 °C / Inert atmosphere

10: n-butyllithium / tetrahydrofuran; hexane; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -100 °C / Inert atmosphere

With 4-methyl-morpholine; 2,6-dimethylpyridine; tert.-butylhydroperoxide; n-butyllithium; samarium diiodide; boron trifluoride diethyl etherate; potassium tert-butylate; diisobutylaluminium hydride; lithium triethylborohydride; sodium hydrogencarbonate; triethylamine; lithium chloride; methyl iodide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; water; acetonitrile; 8: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/ol500788c

Reference yield:

: methyl 3-O-benzyl-2,5-dideoxy-D-erythropentofuranoside

: 1592771-29-3
C₅₅H₇₈O₁₀SSi₂

Guidance literature:: Multi-step reaction with 12 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 - 20 °C / Inert atmosphere

2: 4-methyl-morpholine / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 24 h / 20 °C

4: samarium diiodide / acetonitrile; methanol / 1 h / -20 °C / Inert atmosphere

5: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

6: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / -80 °C / Inert atmosphere

7: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

8: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

9: diisobutylaluminium hydride / dichloromethane; hexane / 0.75 h / -80 °C / Inert atmosphere

10: lithium chloride; triethylamine / acetonitrile / 5 h / 20 °C / Inert atmosphere

11: potassium tert-butylate; tert.-butylhydroperoxide / tetrahydrofuran / 16 h / -80 - -25 °C / Inert atmosphere

12: n-butyllithium / tetrahydrofuran; hexane; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -100 °C / Inert atmosphere

With 4-methyl-morpholine; 2,6-dimethylpyridine; tert.-butylhydroperoxide; sodium tetrahydroborate; n-butyllithium; samarium diiodide; boron trifluoride diethyl etherate; potassium tert-butylate; potassium hexamethylsilazane; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; lithium chloride; methyl iodide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; water; toluene; acetonitrile; 5: |Dess-Martin Oxidation / 10: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/ol500788c