2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran

Base Information

Chemical Name:2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran
CAS No.:1415636-40-6
Molecular Formula:C₃₉H₄₉IO₄
Molecular Weight:708.72
Hs Code.:

Synonyms:2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran

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Chemical Property of 2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran

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Technology Process of 2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran

There total 3 articles about 2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1415636-39-3
3,3'-bis(heptyloxy)-4,4'-diiodobiphenyl

: 119754-16-4
[4-(tetrahydropyran-2-yloxy)phenyl]ethyne

: 1415636-40-6
2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 25 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201203014

Reference yield:

: 678988-82-4
4,4'-diiodo-3,3'-dihydroxybiphenyl

: 1415636-40-6
2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

2: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 12 h / 25 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/chem.201203014

Reference yield:

: 629-04-9
1-Bromoheptane

: 1415636-40-6
2-(4-((3,3'-bis(heptyloxy)-4'-iodo biphenyl-4-yl)ethynyl)phenoxy)tetrahydro-2Hpyran

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

2: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 12 h / 25 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/chem.201203014