N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone

Base Information

Chemical Name:N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone
CAS No.:302587-06-0
Molecular Formula:C₂₅H₂₉NO₆
Molecular Weight:439.508
Hs Code.:

Synonyms:N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone

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Technology Process of N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone

There total 3 articles about N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 65047-63-4
2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthol

: 88-10-8
N,N-diethylcarbamyl chloride

: 302587-06-0
N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone

Guidance literature:: With pyridine; at 110 ℃; for 108h;
DOI:10.1016/S0040-4020(00)00551-2

Reference yield:

: 58-74-2
Papaverine

: 302587-06-0
N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / acetone / 72 h / 20 °C

2: 85 percent / NaOH / methanol / 20 h / Heating

3: 75 percent / pyridine / 108 h / 110 °C

With pyridine; sodium hydroxide; In methanol; acetone; 1: Alkylation / 2: Ring cleavage / 3: Acylation;
DOI:10.1016/S0040-4020(00)00551-2

Reference yield:

: 2679-26-7
2-Methylpapaverinium iodide

: 302587-06-0
N,N-diethylamino-2-(3',4'-dimethoxyphenyl)-6,7-dimethoxy-1-naphthyloxymrthanone

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaOH / methanol / 20 h / Heating

2: 75 percent / pyridine / 108 h / 110 °C

With pyridine; sodium hydroxide; In methanol; 1: Ring cleavage / 2: Acylation;
DOI:10.1016/S0040-4020(00)00551-2