1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil

Base Information

Chemical Name:1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil
CAS No.:1051366-20-1
Molecular Formula:C₃₂H₃₀N₂O₇
Molecular Weight:554.599
Hs Code.:

Synonyms:1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil

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Technology Process of 1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil

There total 4 articles about 1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1051366-19-8
1-(2,3-O-isopropylidene-6-O-trityl-α-D-mannopyranosyl)uracil

: 1051366-20-1
1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil

Guidance literature:: With dipyridinium dichromate; acetic anhydride; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/j.ejmech.2007.10.014

Reference yield:

: 83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5
D-Mannose pentaacetate

: 1051366-20-1
1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilyl trifluoromethanesulfonate / acetonitrile

2: toluene-4-sulfonic acid / water

3: pyridinium dichromate; acetic anhydride / dichloromethane

With pyridinium dichromate; trimethylsilyl trifluoromethanesulfonate; acetic anhydride; toluene-4-sulfonic acid; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.carres.2012.10.012

Reference yield:

: 1051366-17-6
1-(α-D-mannopyranosyl)uracil

: 1051366-20-1
1-(2,3-O-isopropylidene-6-O-trityl-α-D-lyxo-hexopyranosyl-4-ulose)uracil

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / water

2: pyridinium dichromate; acetic anhydride / dichloromethane

With pyridinium dichromate; acetic anhydride; toluene-4-sulfonic acid; In dichloromethane; water;
DOI:10.1016/j.carres.2012.10.012