4-bromo-2-[methoxy[(1-[t-butyldiphenylsilyl-oxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]thiophene

Base Information

Chemical Name:4-bromo-2-[methoxy[(1-[t-butyldiphenylsilyl-oxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]thiophene
CAS No.:1239339-94-6
Molecular Formula:C₃₀H₄₁BrO₃SSi₂
Molecular Weight:617.795
Hs Code.:

Synonyms:4-bromo-2-[methoxy[(1-[t-butyldiphenylsilyl-oxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]thiophene

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Chemical Property of 4-bromo-2-[methoxy[(1-[t-butyldiphenylsilyl-oxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]thiophene

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Technology Process of 4-bromo-2-[methoxy[(1-[t-butyldiphenylsilyl-oxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]thiophene

There total 1 articles about 4-bromo-2-[methoxy[(1-[t-butyldiphenylsilyl-oxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1239339-90-2
C₆H₆BrClOS

: 1239339-82-2
1-(t-butyldiphenylsilyloxy)-3-((trimethylsilyl)methyl)but-3-en-2-ol

: 1239339-94-6
4-bromo-2-[methoxy[(1-[t-butyldiphenylsilyl-oxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]thiophene

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0cc00467g

Reference yield:

: 1239339-94-6
4-bromo-2-[methoxy[(1-[t-butyldiphenylsilyl-oxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]thiophene

: 3-bromo-5-(5-((t-butyldiphenylsilyloxy)methyl)-4-methylenetetrahydrofuran-2-yl)thiophene

: 3-bromo-5-(5-((t-butyldiphenylsilyloxy)methyl)-4-methylenetetrahydrofuran-2-yl)thiophene

Guidance literature:: With trimethylsilyl bis(trifluoromethanesulfonyl)imide; In dichloromethane; at -78 ℃; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c0cc00467g