methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate

Base Information

Chemical Name:methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate
CAS No.:116787-77-0
Molecular Formula:C₂₃H₂₆N₂O₅
Molecular Weight:410.47
Hs Code.:

Synonyms:methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate

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Chemical Property of methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate

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Technology Process of methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate

There total 1 articles about methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 106140-31-2
methyl 1-benzyl-4-piperidineacetoacetate

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 116787-77-0
methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate

Guidance literature:: With potassium tert-butylate; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 60 - 70 ℃; for 2h;
DOI:10.1016/S0040-4020(01)90353-9

Reference yield: 86.0%

: 116787-77-0
methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate

: 116787-78-1
1-(1-benzyl-4-piperydyl)-3-(o-nitrophenyl)-2-propanone

Guidance literature:: With hydrogenchloride; for 3h; Heating;
DOI:10.1016/S0040-4020(01)90353-9

Reference yield:

: 116787-77-0
methyl 1-benzyl-α-(o-nitrophenyl)-4-piperidineacetoacetate

: 99878-61-2
2-benzyl-1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / 3 N HCl / 3 h / Heating

2: 70 percent / 1.) m-chlorobenzoic acid; 2.) trifluoroacetic anhydride / CH₂Cl₂; H₂O / 1.) 0 deg C, 1 h; 2.) -15 deg C, 1h, up to rt, 15 min

3: 38 percent / p-toluenesulfonic acid monohydrate / toluene / 22 h / Heating

4: 70 percent / iron powder, acetic acid / ethanol; H₂O / 2 h / Heating

With hydrogenchloride; iron; toluene-4-sulfonic acid; acetic acid; trifluoroacetic anhydride; 3-chlorobenzoate; In ethanol; dichloromethane; water; toluene;
DOI:10.1016/S0040-4020(01)90353-9