diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate

Base Information

Chemical Name:diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate
CAS No.:97280-31-4
Molecular Formula:C₂₉H₃₄N₆O₆
Molecular Weight:562.626
Hs Code.:

diethyl N-<4-<N-<(2-amino-4-hydroxy-6-quinazolinyl)methyl>-N-(3-cyanopropyl)amino>benzoyl>-L-glutamate

Synonyms:diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate

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Chemical Property of diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate

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Technology Process of diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate

There total 4 articles about diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 143-33-9,25596-52-5
sodium cyanide

: 97280-33-6
diethyl N-<4--N-(3-bromopropyl)amino>benzoyl>-L-glutamate

: 97280-31-4
diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate

Guidance literature:: In dimethyl sulfoxide; for 4h; Ambient temperature;
DOI:10.1021/jm00148a016

Reference yield:

: 13726-52-8
diethyl N-(p-aminobenzoyl)-L-glutamate

: 97280-31-4
diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 3 steps

1: 16.5 percent / 2,6-lutidine / N,N-dimethyl-acetamide / 12 h / 100 °C

2: 65 percent / CaCO₃ / N,N-dimethyl-acetamide / 66 h / 25 °C

3: 88 percent / dimethylsulfoxide / 4 h / Ambient temperature

With 2,6-dimethylpyridine; calcium carbonate; In N,N-dimethyl acetamide; dimethyl sulfoxide;
DOI:10.1021/jm00148a016

Reference yield:

: 77766-62-2
2-amino-6-(bromomethyl)-4-hydroxyquinazoline hydrobromide

: 97280-31-4
diethyl N-<4--N-(3-cyanopropyl)amino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / CaCO₃ / N,N-dimethyl-acetamide / 66 h / 25 °C

2: 88 percent / dimethylsulfoxide / 4 h / Ambient temperature

With calcium carbonate; In N,N-dimethyl acetamide; dimethyl sulfoxide;
DOI:10.1021/jm00148a016