N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine

Base Information

Chemical Name:N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine
CAS No.:1361989-91-4
Molecular Formula:C₂₆H₃₆N₂Si₂
Molecular Weight:432.756
Hs Code.:

Synonyms:N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine

Suppliers and Price of N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine

Chemical Property:

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Technology Process of N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine

There total 2 articles about N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: N,N'-di(4-bromophenyl)-N,N'-dimethylethylenediamine

: 1066-54-2
trimethylsilylacetylene

: 1361989-91-4
N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine

Guidance literature:: With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine; for 16h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201102032

Reference yield:

: 7025-95-8
N,N'-dimethyl-N,N'-diphenylethylenediamine

: 1361989-91-4
N,N'-bis(4-(2-trimethylsilyl)ethynylphenyl)-N,N'-dimethylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / chloroform / 2 h / 0 °C

2: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / 16 h / Inert atmosphere; Reflux

With piperidine; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; triphenylphosphine; In chloroform;
DOI:10.1002/chem.201102032