(+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene

Base Information

• Chemical Name: (+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene
• CAS No.: 93084-46-9
• Molecular Formula: C₂₀H₂₆N₂O₄S₂
• Molecular Weight: 422.569

Synonyms:(+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene

Chemical Property of (+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene

There total 6 articles about (+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine (93062-04-5) → (+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene (93084-46-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 0.25h; Ambient temperature;

DOI:10.1021/ja00337a037

Reference yield:

N-sulfinyl-p-toluenesulfonamide (4104-47-6) → (+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene (93084-46-9)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine / benzene / 1 h / Ambient temperature

2: 48 percent / benzene / 15 h / Ambient temperature

3: 100 percent / benzene / 1 h / Heating

4: 94 percent / NaBH₄ / methanol / 0.25 h / Ambient temperature

With pyridine; sodium tetrahydroborate; In methanol; benzene;

DOI:10.1021/ja00337a037

Reference yield:

bis(p-toluenesulfonyl) sulfur diimide (851-06-9) → (+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene (93084-46-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 48 percent / benzene / 15 h / Ambient temperature

2: 100 percent / benzene / 1 h / Heating

3: 94 percent / NaBH₄ / methanol / 0.25 h / Ambient temperature

With sodium tetrahydroborate; In methanol; benzene;

DOI:10.1021/ja00337a037

upstream raw materials:

(+/-)-<3α,4β(E)>-2,5-bis<(4-methylphenyl)sulfonyl>-3-methyl-4-(1-propenyl)-1,2,5-thiadiazolidine

C₂₆H₃₀N₂O₄S₃

3,6-dimethyl-2-(toluene-4-sulfonyl)-1-(toluene-4-sulfonylimino)-1,2,3,6-tetrahydro-1λ⁴-[1,2]thiazine

N-[(3R,6S)-3,6-Dimethyl-2-(toluene-4-sulfonyl)-3,6-dihydro-2H-1λ⁴-[1,2]thiazin-(1E)-ylidene]-4-methyl-benzenesulfonamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 93084-46-9 (+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene

Send

Send

Metric Ton KG G Pound L ML

Send

Send