8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine

Base Information

Chemical Name:8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine
CAS No.:873106-43-5
Molecular Formula:C₂₆H₂₁N₃S₂
Molecular Weight:439.605
Hs Code.:

Synonyms:8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine

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Technology Process of 8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine

There total 3 articles about 8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 873106-29-7
5-amino-4,6-bis(p-tolylthio)pyrimidine

: 99-94-5
p-Toluic acid

: 873106-43-5
8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine

Guidance literature:: With trichlorophosphate; for 15h; Heating;
DOI:10.1021/jo051873k

Reference yield: 96.0%

: 873106-43-5
8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine

Guidance literature:

Reference yield:

: 106-45-6
para-thiocresol

: 873106-43-5
8-methyl-6-(p-tolyl)-4-(p-tolylthio)benzo[f]pyrimido[4,5-b][1,4]thiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / triethylamine / butan-1-ol / Heating

2: 97 percent / PPA; POCl₃ / 15 h / Heating

With triethylamine; trichlorophosphate; In butan-1-ol;
DOI:10.1021/jo051873k