(2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

Base Information

Chemical Name:(2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane
CAS No.:866429-74-5
Molecular Formula:C₄₀H₆₄O₁₀
Molecular Weight:704.942
Hs Code.:

Synonyms:(2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

Suppliers and Price of (2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

There total 6 articles about (2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 866429-89-2
1,4-bis-O-(6-benzyloxyhexyl)-2,3-bis-O-(2-hydroxyethyl)-D-threitol

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 866429-74-5
(2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

Guidance literature:: 1,4-bis-O-(6-benzyloxyhexyl)-2,3-bis-O-(2-hydroxyethyl)-D-threitol; In tetrahydrofuran; at 80 ℃; for 2h;

triethylene glycol di-(p-toluenesulfonate); In tetrahydrofuran; at 80 ℃; for 48h;
DOI:10.1016/j.tetasy.2005.06.039

Reference yield:

: 866429-87-0
1,4-bis-O-(6-benzyloxyhexyl)-D-threitol

: 866429-74-5
(2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 2 h / 80 °C

1.2: 36 percent / tetrahydrofuran / 48 h / 80 °C

2.1: 91 percent / aq. HCl / ethanol / 3 h / Heating

3.1: tetrahydrofuran / 2 h / 80 °C

3.2: 25 percent / tetrahydrofuran / 48 h / 80 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tetasy.2005.06.039

Reference yield:

: 866429-85-8
1,4-bis-O-(6-benzyloxyhexyl)-2,3-O-isopropylidene-D-threitol

: 866429-74-5
(2R,3R)-2,3-Bis-(6-benzyloxy-hexyloxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

Guidance literature:: Multi-step reaction with 4 steps

1.1: 90 percent / aq. HCl / methanol / 4 h / 20 °C

2.1: NaH / tetrahydrofuran / 2 h / 80 °C

2.2: 36 percent / tetrahydrofuran / 48 h / 80 °C

3.1: 91 percent / aq. HCl / ethanol / 3 h / Heating

4.1: tetrahydrofuran / 2 h / 80 °C

4.2: 25 percent / tetrahydrofuran / 48 h / 80 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran; methanol; ethanol;
DOI:10.1016/j.tetasy.2005.06.039