Technology Process of C14H18O2
There total 3 articles about C14H18O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hydroxide monohydrate; dihydrogen peroxide / tetrahydrofuran; water / 6 h / 20 °C / Inert atmosphere
2: pyridine; benzenesulfonyl chloride / 12 h / 0 - 35 °C / Inert atmosphere
With
pyridine; lithium hydroxide monohydrate; dihydrogen peroxide; benzenesulfonyl chloride;
In
tetrahydrofuran; water;
DOI:10.1002/anie.201202643
- Guidance literature:
-
With
pyridine; benzenesulfonyl chloride;
at 0 - 35 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/anie.201202643
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 0.25 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 - 0 °C / Inert atmosphere
1.3: 2.5 h / -78 - -10 °C / Inert atmosphere
2.1: lithium hydroxide monohydrate; dihydrogen peroxide / tetrahydrofuran; water / 6 h / 20 °C / Inert atmosphere
3.1: pyridine; benzenesulfonyl chloride / 12 h / 0 - 35 °C / Inert atmosphere
With
pyridine; lithium hydroxide monohydrate; di-n-butylboryl trifluoromethanesulfonate; dihydrogen peroxide; benzenesulfonyl chloride;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1002/anie.201202643
