8-(2,3,4,5-tetramethyl-1,3-cyclopentadienyl)-1,2,3,4-tetrahydroquinoline

Base Information

Chemical Name:8-(2,3,4,5-tetramethyl-1,3-cyclopentadienyl)-1,2,3,4-tetrahydroquinoline
CAS No.:1003295-00-8
Molecular Formula:C₁₈H₂₃N
Molecular Weight:253.387
Hs Code.:

Synonyms:8-(2,3,4,5-tetramethyl-1,3-cyclopentadienyl)-1,2,3,4-tetrahydroquinoline

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Chemical Property of 8-(2,3,4,5-tetramethyl-1,3-cyclopentadienyl)-1,2,3,4-tetrahydroquinoline

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Technology Process of 8-(2,3,4,5-tetramethyl-1,3-cyclopentadienyl)-1,2,3,4-tetrahydroquinoline

There total 2 articles about 8-(2,3,4,5-tetramethyl-1,3-cyclopentadienyl)-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 80673-75-2
2,3,4,5-tetramethylcyclopentene-1-one

: C₁₀H₁₀NO₂^(1-)*Li⁽¹⁺⁾

: 1003295-00-8
8-(2,3,4,5-tetramethyl-1,3-cyclopentadienyl)-1,2,3,4-tetrahydroquinoline

Guidance literature:: C₁₀H₁₀NO₂^(1-)*Li⁽¹⁺⁾; In tetrahydrofuran; diethyl ether; at -20 ℃; for 0.5h; Schlenk technique;

With tert.-butyl lithium; In tetrahydrofuran; diethyl ether; at -20 ℃; for 6h;

2,3,4,5-tetramethylcyclopentene-1-one; With CeCl₃*Cl₂Li₂; In tetrahydrofuran; diethyl ether; at 20 ℃; for 1h; Inert atmosphere;

Reference yield: 40.0%

: 80673-75-2
2,3,4,5-tetramethylcyclopentene-1-one

: 33735-01-2
lithium 1,2,3,4-tetrahydroquinolide

: 1003295-00-8
8-(2,3,4,5-tetramethyl-1,3-cyclopentadienyl)-1,2,3,4-tetrahydroquinoline

Guidance literature:: lithium 1,2,3,4-tetrahydroquinolide; With tetrahydrofuran; In diethyl ether; at -20 ℃; for 0.5h; Schlenk technique; Cooling with acetone-dry ice;

With tert.-butyl lithium; In diethyl ether; at -20 ℃; for 6h;

2,3,4,5-tetramethylcyclopentene-1-one; With cerium(III) chloride bis(lithium chloride); In tetrahydrofuran; diethyl ether; at 20 ℃; for 1h; Inert atmosphere;