C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾
CAS No.:1311411-98-9
Molecular Formula:C₃₀H₃₄FN₂O₆*Na
Molecular Weight:560.598
Hs Code.:

C<sub>30</sub>H<sub>34</sub>FN<sub>2</sub>O<sub>6</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾

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Chemical Property of C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾

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Technology Process of C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾

There total 14 articles about C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1311411-97-8
C₂₄H₂₈BrFNO₅^(1-)*Li⁽¹⁺⁾

: 163105-89-3,600726-67-8
2-methoxy-pyridine-5-boronic acid

: 1311411-98-9
C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾

Guidance literature:: With sodium carbonate; palladium diacetate; In methanol; water; at 40 - 75 ℃; for 0.75h; Inert atmosphere;

Reference yield:

: 27200-79-9
p-bromophenylacetaldehyde

: 1311411-98-9
C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 7 steps

1.1: formic acid / water; methanol / 24 h / 40 °C

2.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.33 h / -78 °C

2.3: -40 °C

3.1: Chiralpak Daicel^.(R). AD-20 / isopropyl alcohol / Resolution of racemate

4.1: hydrogen / tetrahydrofuran / 3 h / 25 °C

5.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

5.2: 1.5 h / -78 °C

6.1: lithium hydroxide / water; methanol / 20 °C

7.1: sodium carbonate / palladium diacetate / water; methanol / 0.75 h / 40 - 75 °C / Inert atmosphere

With n-butyllithium; formic acid; hydrogen; sodium carbonate; diisopropylamine; lithium hydroxide; lithium hexamethyldisilazane; palladium diacetate; In tetrahydrofuran; methanol; water; isopropyl alcohol;

Reference yield:

: 4654-39-1
4-bromophenethanol

: 1311411-98-9
C₃₀H₃₄FN₂O₆^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydrogencarbonate; sodium hypochlorite; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 0 °C

2.1: formic acid / water; methanol / 24 h / 40 °C

3.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

3.2: 0.33 h / -78 °C

3.3: -40 °C

4.1: Chiralpak Daicel^.(R). AD-20 / isopropyl alcohol / Resolution of racemate

5.1: hydrogen / tetrahydrofuran / 3 h / 25 °C

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

6.2: 1.5 h / -78 °C

7.1: lithium hydroxide / water; methanol / 20 °C

8.1: sodium carbonate / palladium diacetate / water; methanol / 0.75 h / 40 - 75 °C / Inert atmosphere

With sodium hypochlorite; n-butyllithium; formic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydrogen; sodium hydrogencarbonate; sodium carbonate; diisopropylamine; sodium bromide; lithium hydroxide; lithium hexamethyldisilazane; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;