2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane

Base Information

Chemical Name:2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane
CAS No.:355017-43-5
Molecular Formula:C₂₆H₁₂N₄O₄S
Molecular Weight:476.472
Hs Code.:

Synonyms:2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane

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Chemical Property of 2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane

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Technology Process of 2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane

There total 3 articles about 2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 109-77-3
malononitrile

: 355017-39-9
4-(9,12-anthraquinone-2-sulfoxy)phenol

: 355017-43-5
2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane

Guidance literature:: With pyridine; titanium tetrachloride; 3-amino propanoic acid; In dichloromethane; for 15h; Heating;
DOI:10.1021/jo001576+

Reference yield:

: 2381-23-9
9,10-dioxo-9,10-dihydro-2-anthracenesulfonyl chloride

: 355017-43-5
2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / pyridine / acetonitrile; CH₂Cl₂ / 20 °C

2: 69 percent / pyridine; TiCl4; β-alanine / CH2Cl2 / 15 h / Heating

With pyridine; titanium tetrachloride; 3-amino propanoic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jo001576+

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 355017-43-5
2-(4-hydroxyphenyloxysulfonyl)-13,13,14,14-tetracyanoanthraquinodimethane

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / pyridine / acetonitrile; CH₂Cl₂ / 20 °C

2: 69 percent / pyridine; TiCl4; β-alanine / CH2Cl2 / 15 h / Heating

With pyridine; titanium tetrachloride; 3-amino propanoic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jo001576+