methyl-4-(1-(4-methyl-N-phenylphenylsulfonamido)-1-oxo-2-(p-tolylthio)pent-4-en-2-yl)benzoate

Base Information

Chemical Name:methyl-4-(1-(4-methyl-N-phenylphenylsulfonamido)-1-oxo-2-(p-tolylthio)pent-4-en-2-yl)benzoate
CAS No.:1609958-98-6
Molecular Formula:C₃₃H₃₁NO₅S₂
Molecular Weight:585.745
Hs Code.:

Synonyms:methyl-4-(1-(4-methyl-N-phenylphenylsulfonamido)-1-oxo-2-(p-tolylthio)pent-4-en-2-yl)benzoate

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Chemical Property of methyl-4-(1-(4-methyl-N-phenylphenylsulfonamido)-1-oxo-2-(p-tolylthio)pent-4-en-2-yl)benzoate

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Technology Process of methyl-4-(1-(4-methyl-N-phenylphenylsulfonamido)-1-oxo-2-(p-tolylthio)pent-4-en-2-yl)benzoate

There total 2 articles about methyl-4-(1-(4-methyl-N-phenylphenylsulfonamido)-1-oxo-2-(p-tolylthio)pent-4-en-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1516-28-5
allyl (p-tolyl)sulfide

: 1609958-85-1
methyl 4-((4-methyl-N-phenylphenylsulfonamido)ethynyl)benzoate

: 1609958-98-6
methyl-4-(1-(4-methyl-N-phenylphenylsulfonamido)-1-oxo-2-(p-tolylthio)pent-4-en-2-yl)benzoate

Guidance literature:: With 1-oxy-pyridine-2-carboxylic acid methyl ester; C₄₄H₆₄AuF₆NO₇PS₂; In dichloromethane; at 23 ℃; for 9h; Inert atmosphere;
DOI:10.1039/c4cc01059k

Reference yield:

: 68-34-8
phenyl toluenesulfonamide

: 3034-86-4
4-ethynylbenzoic acid methyl ester

: 1609958-98-6
methyl-4-(1-(4-methyl-N-phenylphenylsulfonamido)-1-oxo-2-(p-tolylthio)pent-4-en-2-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper dichloride; sodium carbonate; pyridine; oxygen / toluene / 0.25 h / 70 °C

1.2: 8 h / 70 °C

2.1: 1-oxy-pyridine-2-carboxylic acid methyl ester; C₄₄H₆₄AuF₆NO₇PS₂ / dichloromethane / 9 h / 23 °C / Inert atmosphere

With pyridine; 1-oxy-pyridine-2-carboxylic acid methyl ester; C₄₄H₆₄AuF₆NO₇PS₂; oxygen; sodium carbonate; copper dichloride; In dichloromethane; toluene;
DOI:10.1039/c4cc01059k