2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene

Base Information

Chemical Name:2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene
CAS No.:153778-29-1
Molecular Formula:C₂₈H₂₃ClO₃
Molecular Weight:442.942
Hs Code.:

Synonyms:2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene

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Chemical Property of 2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene

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Technology Process of 2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene

There total 5 articles about 2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 151806-60-9
1,1-bis-(4-benzyloxy-phenyl)-2-chloro-2-(4-methoxy-phenyl)-ethene

: 4-[(E)-1-(4-Benzyloxy-phenyl)-2-chloro-2-(4-methoxy-phenyl)-vinyl]-phenol

: 153778-29-1
2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene

Guidance literature:: With hydrogen; acetic acid; 10% palladium on active carbon; In tetrahydrofuran; under 760 Torr; Yield given;
DOI:10.1002/jps.2600820911

Reference yield:

: 16208-17-6
2,2-dihydroxy-1-(4-methoxyphenyl)ethan-1-one

: 153778-29-1
2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / conc. H₂SO₄ / acetic acid / 1.) 3 h, 15 deg C; 2.) overnight, room temp.

2: 77 percent / potassium carbonate / acetone / 8 h / Heating

3: PCl₅ / benzene / 5 h / Heating

4: H₂, glacial acetic acid / Pd/C (10percent Pd) / tetrahydrofuran / 760 Torr

With phosphorus pentachloride; sulfuric acid; hydrogen; potassium carbonate; acetic acid; 10% palladium on active carbon; In tetrahydrofuran; acetic acid; acetone; benzene;
DOI:10.1002/jps.2600820911

Reference yield:

: 153777-97-0
2,2-bis(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethan-1-one

: 153778-29-1
2-(4-benzyloxyphenyl)-1-chloro-2-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-ethene

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / potassium carbonate / acetone / 8 h / Heating

2: PCl₅ / benzene / 5 h / Heating

3: H₂, glacial acetic acid / Pd/C (10percent Pd) / tetrahydrofuran / 760 Torr

With phosphorus pentachloride; hydrogen; potassium carbonate; acetic acid; 10% palladium on active carbon; In tetrahydrofuran; acetone; benzene;
DOI:10.1002/jps.2600820911