[4-[6-amino-5-(1-isopropyltriazol-4-yl)-3-pyridyl]phenyl]morpholinomethanone

Base Information

Chemical Name:[4-[6-amino-5-(1-isopropyltriazol-4-yl)-3-pyridyl]phenyl]morpholinomethanone
CAS No.:1617499-04-3
Molecular Formula:C₂₁H₂₄N₆O₂
Molecular Weight:392.461
Hs Code.:

Synonyms:[4-[6-amino-5-(1-isopropyltriazol-4-yl)-3-pyridyl]phenyl]morpholinomethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [4-[6-amino-5-(1-isopropyltriazol-4-yl)-3-pyridyl]phenyl]morpholinomethanone

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Technology Process of [4-[6-amino-5-(1-isopropyltriazol-4-yl)-3-pyridyl]phenyl]morpholinomethanone

There total 2 articles about [4-[6-amino-5-(1-isopropyltriazol-4-yl)-3-pyridyl]phenyl]morpholinomethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.97%

: 389621-84-5
4-(morpholine-4-carbonyl)phenylboronic acid

: 1617499-16-7
5-bromo-3-(1-isopropyl-1H-[1,2,3]triazol-4-yl)-pyridin-2-ylamine

: 1617499-04-3
[4-[6-amino-5-(1-isopropyltriazol-4-yl)-3-pyridyl]phenyl]morpholinomethanone

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,4-dioxane; water; at 110 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 1210838-82-6
5-bromo-3-ethynyl-pyridin-2-ylamine

: 1617499-04-3
[4-[6-amino-5-(1-isopropyltriazol-4-yl)-3-pyridyl]phenyl]morpholinomethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide / water; tert-butyl alcohol / 2 h / 80 °C

1.2: 16 h / 80 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,4-dioxane; water / 0.5 h / 110 °C / Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; caesium carbonate; In 1,4-dioxane; water; tert-butyl alcohol;