C₁₃H₁₆ClNO₂

Base Information

Chemical Name:C₁₃H₁₆ClNO₂
CAS No.:1269461-39-3
Molecular Formula:C₁₃H₁₆ClNO₂
Molecular Weight:253.729
Hs Code.:

C<sub>13</sub>H<sub>16</sub>ClNO<sub>2</sub>

Synonyms:C₁₃H₁₆ClNO₂

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Chemical Property of C₁₃H₁₆ClNO₂

Chemical Property:

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Technology Process of C₁₃H₁₆ClNO₂

There total 2 articles about C₁₃H₁₆ClNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 1269460-63-0
C₁₂H₁₇NO

: 1269461-39-3
C₁₃H₁₆ClNO₂

: 1269461-23-5
C₁₃H₁₆ClNO₂

Guidance literature:: C₁₂H₁₇NO; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; Inert atmosphere;

bis(trichloromethyl) carbonate; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201001375

Reference yield:

: 104-63-2
N-Benzylethanolamine

: 1269461-39-3
C₁₃H₁₆ClNO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; sodium iodide / acetonitrile / Inert atmosphere; Reflux

2.1: thionyl chloride / dichloromethane / 1 h / Inert atmosphere; Reflux

3.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

5.2: 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; thionyl chloride; potassium tert-butylate; sodium hydride; potassium carbonate; sodium iodide; In tetrahydrofuran; dichloromethane; acetonitrile; mineral oil;
DOI:10.1002/ejoc.201001375