C₃₁H₃₅NO₅

Base Information

Chemical Name:C₃₁H₃₅NO₅
CAS No.:603124-15-8
Molecular Formula:C₃₁H₃₅NO₅
Molecular Weight:501.623
Hs Code.:

C<sub>31</sub>H<sub>35</sub>NO<sub>5</sub>

Synonyms:C₃₁H₃₅NO₅

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Chemical Property of C₃₁H₃₅NO₅

Chemical Property:

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Technology Process of C₃₁H₃₅NO₅

There total 15 articles about C₃₁H₃₅NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132990-84-2
(2S)-N-benzyl-7-methoxy-1,2,3,4-tetrahydronaphthalen-2-amine

: 603124-15-8
C₃₁H₃₅NO₅

Guidance literature:: Multi-step reaction with 9 steps

1: boron tribromide / dichloromethane / 4 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h

3: sodium hydroxide / tetrahydrofuran; water / 1 h / 20 °C / pH 7 - 8

4: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water / 2 h / 20 - 80 °C / Inert atmosphere

6: palladium 10% on activated carbon; hydrogen / methanol / 1 h

7: ethanol / Reflux

8: tetrahydrofuran / 20 °C

9: methanol; sodium hydroxide; water / 20 °C

With 2,6-dimethylpyridine; methanol; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; water; hydrogen; boron tribromide; sodium carbonate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 5: Suzuki coupling;
DOI:10.1021/jm800222k

Reference yield:

: 603122-70-9
(7S)-7-(benzylamino)-5,6,7,8-tetrahydronaphthalen-2-ol

: 603124-15-8
C₃₁H₃₅NO₅

Guidance literature:: Multi-step reaction with 8 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 2 h

2: sodium hydroxide / tetrahydrofuran; water / 1 h / 20 °C / pH 7 - 8

3: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water / 2 h / 20 - 80 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen / methanol / 1 h

6: ethanol / Reflux

7: tetrahydrofuran / 20 °C

8: methanol; sodium hydroxide; water / 20 °C

With 2,6-dimethylpyridine; methanol; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; water; hydrogen; sodium carbonate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 4: Suzuki coupling;
DOI:10.1021/jm800222k

Reference yield:

: 194785-39-2
benzyl [(2S)-7-hydroxy-1,2,3,4-tetrahydronaphthalen-2-yl]carbamate

: 603124-15-8
C₃₁H₃₅NO₅

Guidance literature:: Multi-step reaction with 6 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water / 2 h / 20 - 80 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 1 h

4: ethanol / Reflux

5: tetrahydrofuran / 20 °C

6: methanol; sodium hydroxide; water / 20 °C

With 2,6-dimethylpyridine; methanol; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; water; hydrogen; sodium carbonate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 2: Suzuki coupling;
DOI:10.1021/jm800222k