2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID

Base Information

• Chemical Name: 2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID
• CAS No.: 32403-69-3
• Molecular Formula: C8H6N2O6S
• Molecular Weight: 258.211
• Mol file: 32403-69-3.mol

Synonyms:

Chemical Property of 2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID

Chemical Property:

• Vapor Pressure: 2.4E-09mmHg at 25°C
• Boiling Point: 462.3°C at 760 mmHg
• Flash Point: 233.4°C
• PSA: 154.24000
• Density: 1.66g/cm³
• LogP: 2.72610

Purity/Quality:

98% ^*data from raw suppliers

[(2,4-Dinitrophenyl)thio]acetic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID

There total 7 articles about 2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

mercaptoacetic acid (68-11-1) + 1-chloro-2,4-dinitro-benzene (97-00-7) → 2-(2,4-dinitrophenylthio)acetic acid (32403-69-3)

Guidance literature:

With triethylamine; In 1,4-dioxane; water;

Reference yield:

2-(benzo[d]thiazol-2-yl)phenyl 2,4-dinitrobenzenesulfonate (1373156-67-2) + mercaptoacetic acid (68-11-1) → 2-(benzothiazol-2-yl)phenol (3411-95-8) + 2-(2,4-dinitrophenylthio)acetic acid (32403-69-3)

Guidance literature:

In dimethyl sulfoxide; for 0.5h; pH=7.4; aq. phosphate buffer;

DOI:10.1016/j.tetlet.2012.02.098

Reference yield:

2,4-dinitrothiophenol (2218-96-4) + chloroacetic acid (79-11-8) → 2-(2,4-dinitrophenylthio)acetic acid (32403-69-3)

Guidance literature:

With sodium carbonate; at 80 ℃;

upstream raw materials:

bis(2,4-dinitrophenyl) disulphide

mercaptoacetic acid

1-chloro-2,4-dinitro-benzene

2,4-dinitrothiophenol

Downstream raw materials:

methyl (2,4-dinitrophenylsulphanyl)ethanoate

(2,4-dinitro-benzenesulfonyl)-acetic acid

6-amino-2H-1,4-benzothiazin-3(4H)-one

2,4-dinitrophenylthioglycolic acid N-hydroxy succinimide ester

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