(Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide

Base Information

Chemical Name:(Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide
CAS No.:1596305-99-5
Molecular Formula:C₂₆H₄₀BrNOSi
Molecular Weight:490.599
Hs Code.:

Synonyms:(Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide

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Technology Process of (Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide

There total 3 articles about (Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1596305-82-6
(E)-3-(4-bromophenyl)-N,N-diisopropylacrylamide

: 181934-30-5
1-[(triisopropylsilyl)ethynyl]-1,2-benziodoxol-3(1H)-one

: 1596305-99-5
(Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide

Guidance literature:: With acetonitrile; In dichloromethane; at 80 ℃; for 16h;
DOI:10.1039/c4cc01141d

Reference yield:

: 27465-66-3,13565-09-8
4-bromocinnamoyl chloride

: 1596305-99-5
(Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 20 °C / Inert atmosphere

2: acetonitrile / dichloromethane / 16 h / 80 °C

With acetonitrile; In dichloromethane;
DOI:10.1039/c4cc01141d

Reference yield:

: 1200-07-3,5676-63-1,17916-60-8
trans-4-bromocinnamic acid

: 1596305-99-5
(Z)-3-(4-bromophenyl)-N,N-diisopropyl-5-(triisopropylsilyl)pent-2-en-4-ynamide

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

2: dichloromethane / 2 h / 20 °C / Inert atmosphere

3: acetonitrile / dichloromethane / 16 h / 80 °C

With oxalyl dichloride; acetonitrile; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c4cc01141d