5-(2-bromophenyl)-pent-2-en-4-ynoic acid butyl ester

Base Information

• Chemical Name: 5-(2-bromophenyl)-pent-2-en-4-ynoic acid butyl ester
• CAS No.: 1041003-17-1
• Molecular Formula: C₁₅H₁₅BrO₂
• Molecular Weight: 307.187
• Mol file: 1041003-17-1.mol

Synonyms:5-(2-bromophenyl)-pent-2-en-4-ynoic acid butyl ester

Chemical Property of 5-(2-bromophenyl)-pent-2-en-4-ynoic acid butyl ester

Chemical Property:

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Technology Process of 5-(2-bromophenyl)-pent-2-en-4-ynoic acid butyl ester

There total 1 articles about 5-(2-bromophenyl)-pent-2-en-4-ynoic acid butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

acrylic acid n-butyl ester (141-32-2,9003-49-0) + C8H5BrI2 → 5-(2-bromophenyl)-pent-2-en-4-ynoic acid butyl ester (1041003-17-1)

Guidance literature:

With 4-methyl-morpholine; potassium carbonate; hydroxyapatite-supported palladium(II) complex; at 90 ℃; for 4.5h;

DOI:10.1021/jo800209z

upstream raw materials:

acrylic acid n-butyl ester