C₃₄H₅₉Si₂NO₇

Base Information

Chemical Name:C₃₄H₅₉Si₂NO₇
CAS No.:937164-17-5
Molecular Formula:C₃₄H₅₉NO₇Si₂
Molecular Weight:650.016
Hs Code.:

C<sub>34</sub>H<sub>59</sub>Si<sub>2</sub>NO<sub>7</sub>

Synonyms:C₃₄H₅₉Si₂NO₇

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Chemical Property of C₃₄H₅₉Si₂NO₇

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Technology Process of C₃₄H₅₉Si₂NO₇

There total 7 articles about C₃₄H₅₉Si₂NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 937163-73-0
C₁₇H₃₄SiO₄

: 937164-17-5
C₃₄H₅₉Si₂NO₇

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

2: 82 percent / NIS / CH₂Cl₂ / 20 °C

3: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

4: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

With N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ol070435s

Reference yield:

: 937164-11-9
C₂₄H₃₈SiO₅

: 937164-17-5
C₃₄H₅₉Si₂NO₇

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / DIBAL-H / CH₂Cl₂ / 1 h / -78 °C

2: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

3: 82 percent / NIS / CH₂Cl₂ / 20 °C

4: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

5: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

With N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; diisobutylaluminium hydride; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ol070435s

Reference yield:

: 937164-09-5
C₂₂H₃₄SiO₄

: 937164-17-5
C₃₄H₅₉Si₂NO₇

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / P₂O₅ / 0.5 h / 20 °C

2: 73 percent / DIBAL-H / CH₂Cl₂ / 1 h / -78 °C

3: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

4: 82 percent / NIS / CH₂Cl₂ / 20 °C

5: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

6: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

With N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; phosphorus pentoxide; diisobutylaluminium hydride; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ol070435s