1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

Base Information

Chemical Name:1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate
CAS No.:479404-76-7
Molecular Formula:C₅₄H₇₇O₈P
Molecular Weight:885.174
Hs Code.:

Synonyms:1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

Suppliers and Price of 1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

There total 8 articles about 1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1-[benzyl(2'-butenyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

: 479404-76-7
1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

Guidance literature:: With potassium diazodicarboxylate; acetic acid; In methanol; at 40 ℃;
DOI:10.1021/jo026247r

Reference yield:

: 544-77-4
1-iodohexadecane

: 479404-76-7
1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0.17 h / 20 °C

1.2: 52 percent / dimethylformamide / 1 h / 20 °C

2.1: (PCy₃)2RuCl₂(=CHPh) / CH₂Cl₂ / 3 h / Heating

3.1: 95 percent / dipotassium azodicarboxylate; glacial AcOH / methanol / 40 °C

With Grubbs catalyst first generation; potassium diazodicarboxylate; sodium hydride; acetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo026247r

Reference yield:

: 479404-32-5
1-(allylbenzyl)-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

: 479404-76-7
1-[benzyl(butyl-4'-O-hexadecyl)]-3,4,6-tri-O-benzyl-2,5-anhydro-D-glucityl phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: (PCy₃)2RuCl₂(=CHPh) / CH₂Cl₂ / 3 h / Heating

2: 95 percent / dipotassium azodicarboxylate; glacial AcOH / methanol / 40 °C

With Grubbs catalyst first generation; potassium diazodicarboxylate; acetic acid; In methanol; dichloromethane;
DOI:10.1021/jo026247r