C₂₁H₂₄ClIN₄O₃

Base Information

Chemical Name:C₂₁H₂₄ClIN₄O₃
CAS No.:1373165-38-8
Molecular Formula:C₂₁H₂₄ClIN₄O₃
Molecular Weight:542.804
Hs Code.:

C<sub>21</sub>H<sub>24</sub>ClIN<sub>4</sub>O<sub>3</sub>

Synonyms:C₂₁H₂₄ClIN₄O₃

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Chemical Property of C₂₁H₂₄ClIN₄O₃

Chemical Property:

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Technology Process of C₂₁H₂₄ClIN₄O₃

There total 12 articles about C₂₁H₂₄ClIN₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 1373165-38-8
C₂₁H₂₄ClIN₄O₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 0 - 20 °C

2.1: dmap / acetonitrile / 8 h / 20 °C

3.1: lithium triethylborohydride / tetrahydrofuran; toluene / -55 - -47 °C

3.2: -50 - -47 °C

3.3: 16 h / -52 - 20 °C

4.1: diethylzinc / toluene / 20 h / -35 - -21 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

6.1: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 2 h / 18 - 24 °C

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C / Inert atmosphere

7.2: 6 h / 98 - 102 °C / Inert atmosphere

7.3: 45 - 52 °C / Inert atmosphere

8.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

9.1: N-chloro-succinimide / acetonitrile / 7 h / 72 - 77 °C / Inert atmosphere

With 1H-imidazole; dmap; sodium periodate; N-chloro-succinimide; tetrabutyl ammonium fluoride; diethylzinc; lithium triethylborohydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; ruthenium trichloride; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 1373165-37-7
C₂₁H₂₅IN₄O₃

: 1373165-38-8
C₂₁H₂₄ClIN₄O₃

Guidance literature:: With N-chloro-succinimide; In acetonitrile; at 72 - 77 ℃; for 7h; Inert atmosphere;

Reference yield:

: 138629-30-8,138871-56-4
(S)-tert-butyl 2-((tert-butyldiphenylsilyloxy)methyl)-5-oxopyrrolidine-1-carboxylate

: 1373165-38-8
C₂₁H₂₄ClIN₄O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium triethylborohydride / tetrahydrofuran; toluene / -55 - -47 °C

1.2: -50 - -47 °C

1.3: 16 h / -52 - 20 °C

2.1: diethylzinc / toluene / 20 h / -35 - -21 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

4.1: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 2 h / 18 - 24 °C

5.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C / Inert atmosphere

5.2: 6 h / 98 - 102 °C / Inert atmosphere

5.3: 45 - 52 °C / Inert atmosphere

6.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

7.1: N-chloro-succinimide / acetonitrile / 7 h / 72 - 77 °C / Inert atmosphere

With sodium periodate; N-chloro-succinimide; tetrabutyl ammonium fluoride; diethylzinc; lithium triethylborohydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; ruthenium trichloride; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;