2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene

Base Information

Chemical Name:2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene
CAS No.:1383782-66-8
Molecular Formula:C₄₄H₃₄BrNS₂
Molecular Weight:720.797
Hs Code.:

Synonyms:2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene

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Chemical Property of 2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene

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Technology Process of 2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene

There total 6 articles about 2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 503475-44-3
2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-5,5'-bisthiophene

: 1383782-66-8
2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene

Guidance literature:: With N-Bromosuccinimide; In chloroform; at 20 ℃; for 1h;
DOI:10.1002/chem.201200020

Reference yield:

: 313050-71-4
N-(4-bromophenyl)-N-(9,9-dimethyl-9H-fluoren-2-yl)-9,9-dimethyl-9H-fluoren-2-amine

: 1383782-66-8
2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 20 h / Inert atmosphere; Reflux

2: N-Bromosuccinimide / chloroform / 1 h / 20 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; chloroform; water; 1: Suzuki coupling;
DOI:10.1002/chem.201200020

Reference yield:

: 479719-88-5
2-([2,2'-bithiophen]-5-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1383782-66-8
2-[N,N-bis-(9,9-dimethylfluoren-2-yl)aminophenyl]-2'-bromo-5,5'-bisthiophene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 1,4-dioxane / 85 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.25 h / 0 - 5 °C

With N-Bromosuccinimide; sodium hydroxide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In 1,4-dioxane; N,N-dimethyl-formamide;