10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione

Base Information

Chemical Name:10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione
CAS No.:388574-96-7
Molecular Formula:C₁₇H₁₄N₄O₂
Molecular Weight:306.324
Hs Code.:

10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-<i>c</i>][1,2,4]triazine-3,4-dione

Synonyms:10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione

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Chemical Property of 10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione

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Technology Process of 10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione

There total 4 articles about 10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 95-92-1
oxalic acid diethyl ester

: 388574-80-9
[1-(4-methyl-benzyl)-1H-benzoimidazol-2-yl]-hydrazine

: 388574-96-7
10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione

Guidance literature:: In ethanol; Heating;
DOI:10.1021/jm0109210

Reference yield:

: 4857-06-1
2-chloro-1H-benzoimidazole

: 388574-96-7
10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide

1.2: 85 percent / dimethylformamide / 20 °C

2.1: 56 percent / hydrazine hydrate / 5 h / 160 °C

3.1: 62 percent / ethanol / Heating

With sodium hydride; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0109210

Reference yield:

: 104-82-5
4-Methylbenzyl chloride

: 388574-96-7
10-(4-methyl-benzyl)-2,10-dihydro-benzo[4,5]imidazo[2,1-c][1,2,4]triazine-3,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide

1.2: 85 percent / dimethylformamide / 20 °C

2.1: 56 percent / hydrazine hydrate / 5 h / 160 °C

3.1: 62 percent / ethanol / Heating

With sodium hydride; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0109210