C₃₅H₃₆O₁₀

Base Information

Chemical Name:C₃₅H₃₆O₁₀
CAS No.:1443651-25-9
Molecular Formula:C₃₅H₃₆O₁₀
Molecular Weight:616.665
Hs Code.:

C<sub>35</sub>H<sub>36</sub>O<sub>10</sub>

Synonyms:C₃₅H₃₆O₁₀

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Chemical Property of C₃₅H₃₆O₁₀

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Technology Process of C₃₅H₃₆O₁₀

There total 15 articles about C₃₅H₃₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: C₂₃H₂₁BF₃O₈^(1-)*K⁽¹⁺⁾

: 139540-24-2
(E)-1-(3'-bromo-but-2'-enyloxymethyl)-4-methoxy-benzene

: 1443651-25-9
C₃₅H₃₆O₁₀

Guidance literature:: C₂₃H₂₁BF₃O₈^(1-)*K⁽¹⁺⁾; With chloro-trimethyl-silane; In tetrahydrofuran; water; at 20 ℃; for 0.333333h;

(E)-1-(3'-bromo-but-2'-enyloxymethyl)-4-methoxy-benzene; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In tetrahydrofuran; water; at 70 ℃; for 4h;
DOI:10.1002/chem.201204545

Reference yield:

: 1443651-22-6
C₁₉H₂₂O₆

: 1443651-25-9
C₃₅H₃₆O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydrochloride monohydrate / tetrahydrofuran; water / 18 h / 20 °C

2.1: 12 h / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 0 - 20 °C / Inert atmosphere

3.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tetrahydrofuran; cyclohexane / 0.25 h / 20 °C / Inert atmosphere

3.2: 48 h / 85 °C / Inert atmosphere

4.1: tetrahydrofuran; water / 7 h / 20 °C

5.1: chloro-trimethyl-silane / tetrahydrofuran; water / 0.33 h / 20 °C

5.2: 4 h / 70 °C

With chloro-trimethyl-silane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; lithium hydrochloride monohydrate; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; cyclohexane; water; 5.2: |Suzuki Coupling;
DOI:10.1002/chem.201204545

Reference yield:

: 1443651-21-5
C₂₃H₃₀O₆

: 1443651-25-9
C₃₅H₃₆O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: boron tribromide / dichloromethane / 12 h / -78 - 20 °C / Inert atmosphere

2.1: lithium hydrochloride monohydrate / tetrahydrofuran; water / 18 h / 20 °C

3.1: 12 h / 0 - 20 °C / Inert atmosphere

3.2: 3 h / 0 - 20 °C / Inert atmosphere

4.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / tetrahydrofuran; cyclohexane / 0.25 h / 20 °C / Inert atmosphere

4.2: 48 h / 85 °C / Inert atmosphere

5.1: tetrahydrofuran; water / 7 h / 20 °C

6.1: chloro-trimethyl-silane / tetrahydrofuran; water / 0.33 h / 20 °C

6.2: 4 h / 70 °C

With chloro-trimethyl-silane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; lithium hydrochloride monohydrate; boron tribromide; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; dichloromethane; cyclohexane; water; 6.2: |Suzuki Coupling;
DOI:10.1002/chem.201204545