(S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate

Base Information

Chemical Name:(S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate
CAS No.:1184944-95-3
Molecular Formula:C₁₁H₁₃NO₃*C₁₁H₁₇NO₂
Molecular Weight:402.491
Hs Code.:

Synonyms:(S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate

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Chemical Property of (S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate

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Technology Process of (S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate

There total 4 articles about (S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 10172-89-1
(R)-N-acetylphenylalanin

: 55707-43-2
1-benzyl-2,2-dimethoxyethylamine

: C₁₁H₁₃NO₃*C₁₁H₁₇NO₂

: 1184944-95-3
(S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate

Guidance literature:: In isopropyl alcohol; at 40 - 50 ℃; for 5h;

Reference yield:

: 1084820-37-0
1,1-dimethoxy-3-phenylpropan-2-one oxime

: 1184944-95-3
(S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / ethanol

2: isopropyl alcohol / 20 - 50 °C

With hydrogen; In ethanol; isopropyl alcohol;
DOI:10.1007/s00726-011-1117-6

Reference yield:

: 1217341-14-4
C₁₈H₂₃NO₂

: 1184944-95-3
(S)-1-benzyl-2,2-dimethoxyethylammonium N-acetyl-D-phenylalaninate

Guidance literature:: Multi-step reaction with 2 steps

1: 5%-palladium/activated carbon; hydrogen / methanol

2: isopropyl alcohol / 20 - 50 °C

With 5%-palladium/activated carbon; hydrogen; In methanol; isopropyl alcohol;
DOI:10.1007/s00726-011-1117-6