benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate

Base Information

Chemical Name:benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate
CAS No.:1040363-77-6
Molecular Formula:C₃₅H₄₇N₃O₇
Molecular Weight:621.774
Hs Code.:

Synonyms:benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate

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Chemical Property of benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate

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Technology Process of benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate

There total 2 articles about benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5781-53-3
monomethyl oxalyl chloride

: 1040363-75-4
benzyl 1-(4-(2-(tert-butoxycarbonylamino)phenylamino)piperidin-1-yl)cyclooctanecarboxylate

: 1040363-77-6
benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate

Guidance literature:: monomethyl oxalyl chloride; benzyl 1-(4-(2-(tert-butoxycarbonylamino)phenylamino)piperidin-1-yl)cyclooctanecarboxylate; In dichloromethane; at 0 ℃; for 0.5h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield: 98.0%

: 1040363-77-6
benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate

Guidance literature:

Reference yield: 76.0%

: 1040363-77-6
benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate

: 1040363-31-2
benzyl 1-(4-(2,3-dioxo-3,4-dihydroquinoxalin-1(2H)-yl)piperidin-1-yl)cyclooctanecarboxylate

Guidance literature:: benzyl 1-(4-(N-(2-(tert-butoxycarbonylamino)phenyl)-2-methoxy-2-oxoacetamido)piperidin-1-yl)cyclooctanecarboxylate; With hydrogenchloride; In ethyl acetate; at 0 - 25 ℃; for 0.5h;

With sodium hydrogencarbonate; In water; ethyl acetate; at 25 ℃; for 0.5h; pH=> 8; Product distribution / selectivity;