dihydro-α-ionone

Base Information

• Chemical Name: dihydro-α-ionone
• CAS No.: 98633-46-6
• Molecular Formula: C₁₃H₂₂O
• Molecular Weight: 194.317

Synonyms:dihydro-α-ionone

Chemical Property of dihydro-α-ionone

Chemical Property:

Purity/Quality:

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Technology Process of dihydro-α-ionone

There total 10 articles about dihydro-α-ionone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(E)-β-ionone (79-77-6,14901-07-6) → dihydro-α-ionone (98633-46-6)

Guidance literature:

With hydrido(triphenylphosphine)copper(I) hexamer; phenylsilane; In toluene; for 47h; Ambient temperature;

DOI:10.1016/S0040-4039(98)00855-7

Reference yield: 82.0%

(E)-β-ionone (79-77-6,14901-07-6) → 4-(2,6,6-Trimethyl-cyclohex-1-enyl)-butan-2-on (17283-81-7) + 4-(2,2,6-trimethylcyclohexyl)-butan-2-one (52612-51-8,52612-53-0,60761-23-1,64666-26-8,6138-85-8) + dihydro-α-ionone (98633-46-6)

Guidance literature:

With ammonium hypophosphorous acid; palladium on activated charcoal; for 12h;

Reference yield: 70.4%

→ dihydro-α-ionone (98633-46-6)

Guidance literature:

upstream raw materials:

(1R,6S)-2,2,6-trimethylcyclohexyl carbaldehyde

acetone

(E)-β-ionone

1-Aethoxymethyl-2,2,6-trimethyl-cyclohexanol-⁽¹⁾

Downstream raw materials:

(E)-4-Oxo-2-[(E)-2-(2,2,6-trimethyl-cyclohexyl)-vinyl]-but-2-enoic acid methyl ester

4-(3-chloro-2-methylidene-6,6-dimethyl-cyclohex-1-yl)-butan-2-one

4-(5-bromo-6-methylene-2,2-dimethylcyclohexyl)-2-butanone

(+/-)-4t-(2.2.6c-trimethyl-cyclohex-r-yl)-but-3-en-2-one-(2.4-dinitro-phenylhydrazone)

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