C₂₄H₄₃NO₇Si

Base Information

Chemical Name:C₂₄H₄₃NO₇Si
CAS No.:1402592-96-4
Molecular Formula:C₂₄H₄₃NO₇Si
Molecular Weight:485.693
Hs Code.:

C<sub>24</sub>H<sub>43</sub>NO<sub>7</sub>Si

Synonyms:C₂₄H₄₃NO₇Si

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Chemical Property of C₂₄H₄₃NO₇Si

Chemical Property:

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Technology Process of C₂₄H₄₃NO₇Si

There total 1 articles about C₂₄H₄₃NO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1402592-68-0
C₁₅H₂₃NO₇

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1402592-96-4
C₂₄H₄₃NO₇Si

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ja308429f

Reference yield:

: 1402592-96-4
C₂₄H₄₃NO₇Si

: 53348-47-3
gliotoxin G

: 67-99-2
gliotoxin

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene / 3 h / 110 °C / Inert atmosphere

2.1: phosphorous acid trimethyl ester / 16 h / 111 °C / Inert atmosphere

3.1: hydrogenchloride / diethyl ether; dichloromethane / 0.25 h / 0 °C / Inert atmosphere

4.1: lithium hydroxide / tetrahydrofuran; water / 5 h / 0 - 25 °C

4.2: pH 3

5.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 15 h / 0 - 25 °C / Inert atmosphere

6.1: dichloromethane / 3 h / 0 - 25 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 15 h / 0 - 25 °C / Inert atmosphere

8.1: sulfur; lithium hexamethyldisilazane / tetrahydrofuran / 2.08 h / 25 °C / Inert atmosphere

With hydrogenchloride; sulfur; 1-hydroxy-7-aza-benzotriazole; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; lithium hydroxide; lithium hexamethyldisilazane; phosphorous acid trimethyl ester; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene;
DOI:10.1021/ja308429f

Reference yield:

: 1402592-96-4
C₂₄H₄₃NO₇Si

: C₃₄H₃₀N₂O₆S₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: toluene / 3 h / 110 °C / Inert atmosphere

2.1: phosphorous acid trimethyl ester / 16 h / 111 °C / Inert atmosphere

3.1: hydrogenchloride / diethyl ether; dichloromethane / 0.25 h / 0 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 4 h / 0 - 25 °C / Inert atmosphere

5.1: sodium hydrogencarbonate / 1,4-dioxane; water / 3.25 h / 0 - 25 °C

6.1: lithium hydroxide / tetrahydrofuran; water / 5 h / 0 - 25 °C

6.2: pH 3

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 17 h / 0 - 25 °C / Inert atmosphere

8.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; diethylamine; 1,4-di(diphenylphosphino)-butane / tetrahydrofuran / 2.05 h / 25 °C / Inert atmosphere

9.1: sulfur; lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 5 h / 25 °C / Inert atmosphere

10.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 5 h / 0 - 25 °C / Inert atmosphere

11.1: 1.3-propanedithiol; triethylamine / dichloromethane; acetonitrile / 0.5 h / 25 °C / Inert atmosphere

With 1.3-propanedithiol; hydrogenchloride; sulfur; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydrogencarbonate; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; 1,4-di(diphenylphosphino)-butane; trifluoroacetic acid; lithium hydroxide; lithium hexamethyldisilazane; phosphorous acid trimethyl ester; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja308429f