(4-methylphenyl)-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilanylamine

Base Information

Chemical Name:(4-methylphenyl)-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilanylamine
CAS No.:1332371-68-2
Molecular Formula:C₂₁H₂₉NSi₂
Molecular Weight:351.639
Hs Code.:

Synonyms:(4-methylphenyl)-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilanylamine

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Chemical Property of (4-methylphenyl)-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilanylamine

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Technology Process of (4-methylphenyl)-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilanylamine

There total 2 articles about (4-methylphenyl)-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilanylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332371-67-1
1-chloro-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilane

: 106-49-0,12221-03-3
p-toluidine

: 1332371-68-2
(4-methylphenyl)-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilanylamine

: 1332371-69-3
C₂₁H₂₉NSi₂

Guidance literature:: p-toluidine; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 3h;

1-chloro-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilane; In tetrahydrofuran; hexane; at -40 - 20 ℃; for 12h; Overall yield = 76 %; Overall yield = 4.80 g;

Reference yield:

: 880652-93-7
4⁽⁷⁾-bromo-2-methyl-1⁽³⁾H-indene

: 1332371-68-2
(4-methylphenyl)-1,1,2,2-tetramethyl-2-(2-methyl-1H-inden-7-yl)disilanylamine

: 1332371-69-3
C₂₁H₂₉NSi₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethylene dibromide; magnesium / tetrahydrofuran / 0.5 h / Reflux

1.2: 14 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / 20 °C

2.2: 12 h / -40 - 20 °C

With n-butyllithium; magnesium; ethylene dibromide; In tetrahydrofuran; hexane;