benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate)

Base Information

Chemical Name:benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate)
CAS No.:109929-97-7
Molecular Formula:C₄₀H₄₇N₃O₄
Molecular Weight:633.831
Hs Code.:

Synonyms:benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate)

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Chemical Property of benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate)

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Technology Process of benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate)

There total 1 articles about benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 16200-52-5
3,4-diethyl-1H-pyrrole

: 3750-36-5
benzyl 5-(acetoxymethyl)-4-ethyl-3-methyl-1H-pyrrole-2-carboxylate

: 109929-97-7
benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate)

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; at 60 ℃; for 8h;
DOI:10.1021/jo00228a048

Reference yield:

: 109929-97-7
benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate)

: C₃₆H₄₀N₄

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen

2: trifluoroacetic acid

With palladium 10% on activated carbon; hydrogen; trifluoroacetic acid;
DOI:10.1039/c3ob41506f

Reference yield:

: 109929-97-7
benzyl 5,5'-(3,4-diethyl-1H-pyrrole-2,5-diyl)bis(methylene)bis(4-ethyl-3-methyl-1H-pyrrole-2-carboxylate)

: C₃₆H₃₈N₄O

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen

2: trifluoroacetic acid

3: silver(I) acetate

With palladium 10% on activated carbon; hydrogen; silver(I) acetate; trifluoroacetic acid;
DOI:10.1039/c3ob41506f