tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate

Base Information

Chemical Name:tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate
CAS No.:1441160-78-6
Molecular Formula:C₂₃H₃₂N₄O₇
Molecular Weight:476.53
Hs Code.:

Synonyms:tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate

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Chemical Property of tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate

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Technology Process of tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate

There total 4 articles about tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1441160-75-3
N-[6-(benzyloxymethyl)-3-oxo-2,5-dihydro-1,2,4-triazin-4-yl]acetamide

: 1441160-78-6
tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate

Guidance literature:: With dmap; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield:

: 1-(benzyloxy)-3-chloropropan-2-one

: 1441160-78-6
tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 16 h / 0 - 20 °C

2: hydrazine hydrate / water; isopropyl alcohol / 24 h / 75 °C

3: dmap / N,N-dimethyl-formamide / 24 h / 20 °C

With dmap; hydrazine hydrate; In water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 13991-52-1,103024-85-7
1-chloro-2-hydroxy-3-phenylmethoxypropane

: 1441160-78-6
tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide; sodium hypochlorite / ethyl acetate; water / 0.5 h / 0 °C

2: N,N-dimethyl-formamide / 16 h / 0 - 20 °C

3: hydrazine hydrate / water; isopropyl alcohol / 24 h / 75 °C

4: dmap / N,N-dimethyl-formamide / 24 h / 20 °C

With dmap; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; hydrazine hydrate; sodium bromide; In water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;