2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone

Base Information

Chemical Name:2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone
CAS No.:171725-18-1
Molecular Formula:C₂₆H₂₂FN₃O₅
Molecular Weight:475.476
Hs Code.:

Synonyms:2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone

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Chemical Property of 2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone

Chemical Property:

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Technology Process of 2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone

There total 4 articles about 2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 393-52-2
2-Fluorobenzoyl chloride

: 171725-18-1
2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / Pd(CH₃CN)2Cl₂ / toluene / 0.5 h / 50 °C

2: 94 percent / 30percent aq. HBr, AcOH / 1 h

3: 2.) Et₃N / 2.) DMF, RT, overnight

With dichloro bis(acetonitrile) palladium(II); hydrogen bromide; acetic acid; triethylamine; In toluene;
DOI:10.1016/S0968-0896(97)00104-1

Reference yield:

: N-(N'-Cbz-glycyl)-2-(tri-n-butylstannyl)aniline

: 171725-18-1
2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / Pd(CH₃CN)2Cl₂ / toluene / 0.5 h / 50 °C

2: 94 percent / 30percent aq. HBr, AcOH / 1 h

3: 2.) Et₃N / 2.) DMF, RT, overnight

With dichloro bis(acetonitrile) palladium(II); hydrogen bromide; acetic acid; triethylamine; In toluene;
DOI:10.1016/S0968-0896(97)00104-1

Reference yield:

: 171725-09-0
2-[N-(N'-Cbz-glycyl)amino]-2'-fluorobenzophenone

: 171725-18-1
2'-fluoro-2-{N-[m-(2-propenyloxycarbonyl)phenyl]ureidomethylcarbamoyl}benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 30percent aq. HBr, AcOH / 1 h

2: 2.) Et₃N / 2.) DMF, RT, overnight

With hydrogen bromide; acetic acid; triethylamine;
DOI:10.1016/S0968-0896(97)00104-1