Technology Process of C24H33NO4
There total 6 articles about C24H33NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H35NO3;
With
H4O6Os(2-)*K(1+); 4-methylmorpholine N-oxide;
In
water; acetone;
With
sodium periodate;
In
tetrahydrofuran; water; acetone;
at 20 ℃;
for 3h;
DOI:10.1021/ja305261h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / N,N-dimethyl-formamide / 20 °C
2.1: sodium triacetoxy borohydride; acetic acid / 1,1-dichloroethane / 12 h / -30 - 20 °C
3.1: H4O6Os(2-)*K(1+); 4-methylmorpholine N-oxide / water; acetone
3.2: 3 h / 20 °C
With
sodium triacetoxy borohydride; H4O6Os(2-)*K(1+); acetic acid; 4-methylmorpholine N-oxide; triethylamine;
In
1,1-dichloroethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja305261h
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C
2.1: lithium perchlorate / dichloromethane / 1 h / 20 °C
3.1: triethylamine / N,N-dimethyl-formamide / 20 °C
4.1: sodium triacetoxy borohydride; acetic acid / 1,1-dichloroethane / 12 h / -30 - 20 °C
5.1: H4O6Os(2-)*K(1+); 4-methylmorpholine N-oxide / water; acetone
5.2: 3 h / 20 °C
With
sodium triacetoxy borohydride; H4O6Os(2-)*K(1+); lithium perchlorate; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; 4-methylmorpholine N-oxide; triethylamine;
In
1,1-dichloroethane; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja305261h
