C₅₃H₉₀O₁₀Si₄

Base Information

Chemical Name:C₅₃H₉₀O₁₀Si₄
CAS No.:817207-79-7
Molecular Formula:C₅₃H₉₀O₁₀Si₄
Molecular Weight:999.634
Hs Code.:

C<sub>53</sub>H<sub>90</sub>O<sub>10</sub>Si<sub>4</sub>

Synonyms:C₅₃H₉₀O₁₀Si₄

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Chemical Property of C₅₃H₉₀O₁₀Si₄

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Technology Process of C₅₃H₉₀O₁₀Si₄

There total 1 articles about C₅₃H₉₀O₁₀Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 36394-07-7
5-hexenoyl chloride

: 1-dimethylsilyl-7,10,13-tris(triethylsilyl)-4,10-deacetyl-4-hydroxybaccatin III

: 817207-79-7
C₅₃H₉₀O₁₀Si₄

Guidance literature:: 1-dimethylsilyl-7,10,13-tris(triethylsilyl)-4,10-deacetyl-4-hydroxybaccatin III; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.75h;

5-hexenoyl chloride; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1021/jm061071x

Reference yield: 88.0%

: 817207-79-7
C₅₃H₉₀O₁₀Si₄

: 817207-83-3
4-deacetyl-4-(5-hexenoyl)-10-deacetylbaccatin III

Guidance literature:: With pyridine; hydrogen fluoride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2004.09.002

Reference yield:

: 817207-79-7
C₅₃H₉₀O₁₀Si₄

: C₅₂H₅₉NO₁₅

Guidance literature:: Multi-step reaction with 7 steps

1: 80 percent / HF*pyridine / tetrahydrofuran / 24 h / 0 - 20 °C

2: 89 percent / CeCl₃ / tetrahydrofuran / 4 h

3: 72 percent / imidazole / CH₂Cl₂ / 3 h / 0 °C

4: 82 percent / lithium hexamethyldisilazide / tetrahydrofuran / 3 h / -40 °C

5: 60 percent / (H₂IMes)(PCy₃)(Cl)2Ru=CHPh / CH₂Cl₂ / 20 °C

6: 78 percent / HF*pyridine / tetrahydrofuran / 0 - 20 °C

7: 65 percent / H₂ / Pd/C / methanol / 6 h / 20 °C / 1810.02 Torr

With 1H-imidazole; cerium(III) chloride; hydrogen; pyridine hydrogenfluoride; lithium hexamethyldisilazane; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm061071x