(dimethylphenylphosphane)gold(I) tert-butylthiolate

Base Information

Chemical Name:(dimethylphenylphosphane)gold(I) tert-butylthiolate
CAS No.:1002113-68-9
Molecular Formula:C₁₂H₂₀AuPS
Molecular Weight:424.297
Hs Code.:

Synonyms:(dimethylphenylphosphane)gold(I) tert-butylthiolate

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Chemical Property of (dimethylphenylphosphane)gold(I) tert-butylthiolate

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Technology Process of (dimethylphenylphosphane)gold(I) tert-butylthiolate

There total 1 articles about (dimethylphenylphosphane)gold(I) tert-butylthiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 77413-77-5
gold(I) 2-methyl-2-propanethiolate

: 672-66-2
Dimethyl(phenyl)phosphine

: 1002113-68-9
(dimethylphenylphosphane)gold(I) tert-butylthiolate

Guidance literature:: In toluene; N2, phosphane (excess) added to a suspn. of Au compd., stirred for 30 min; concd. (vac.), pentane added, ppt. washed (pentane), recrystd. (toluene); elem. anal.;
DOI:10.1002/ejic.200600939

Reference yield: 92.0%

: 1282-37-7
ferrocenium(III) tetrafluoroborate

: 1002113-68-9
(dimethylphenylphosphane)gold(I) tert-butylthiolate

: 102-54-5,55404-68-7
ferrocene

: tetrakis(dimethylphenylphosphane)bis(tert-butylthiolate)tetragold(I) tetrafluoroborate

Guidance literature:: In dichloromethane; byproducts: (SC(CH3)3)2; N2, Fe:Au=0.136:0.276 molar ratio, Fe compd. added to a soln. of Au compd., stirred for 30 min; solvent evapd., residue washed (diethyl ether, benzene), dried (vac.), recrystd. (CH2Cl2, -5°C), org. phases evapd. to dryness, ferrocenesublimied (40°C, high vac.); elem. anal.;
DOI:10.1002/ejic.200600939