5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

Base Information

Chemical Name:5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine
CAS No.:131531-55-0
Molecular Formula:C₄₆H₄₆N₄O₂
Molecular Weight:686.897
Hs Code.:

Synonyms:5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

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Chemical Property of 5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

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Technology Process of 5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

There total 2 articles about 5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5,15-Bis(4-(5,5-dimethyl-1,3-dioxacyclohex-2-yl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

: 131531-55-0
5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

Guidance literature:: With sulfuric acid; In trifluoroacetic acid; for 1h; Ambient temperature;
DOI:10.1002/jhet.5570270626

Reference yield: 42.0%

: 92415-30-0
bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane

: 106456-88-6
4-(5,5-dimethyl-1,3-dioxan-2-yl)benzaldehyde

: 133528-24-2
4-(2',5'-dimethoxybenzyl)benzaldehyde

: 131531-55-0
5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

: 133528-26-4
4-{(1Z,4Z,9Z,15Z)-15-[4-(2,5-Dimethoxy-benzyl)-phenyl]-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin-5-yl}-benzaldehyde

: 133528-25-3
(5Z,10Z,14Z,19Z)-5,15-Bis-[4-(2,5-dimethoxy-benzyl)-phenyl]-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin

Guidance literature:: With sulfuric acid; trifluoroacetic acid; trichloroacetic acid; Yield given. Multistep reaction; 1) acetonitrile;

Reference yield:

: 92415-30-0
bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane

: 17610-00-3
3,5-Di-tert-butylbenzaldehyde

: 131531-55-0
5,15-Bis(4-formylphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

: C₁₃₆H₁₅₈N₁₂

Guidance literature:: With chloranil; trichloroacetic acid; Yield given. Multistep reaction; 1.) acetonitrile, 16 h, 2.) acetonitrile, THF, 4 h;
DOI:10.1246/cl.1993.949