(2,6-di-tert-butylphenyl)hydrogenphenylboronate

Base Information

• Chemical Name: (2,6-di-tert-butylphenyl)hydrogenphenylboronate
• CAS No.: 1037069-91-2
• Molecular Formula: C₂₀H₂₇BO₂
• Molecular Weight: 310.244
• Mol file: 1037069-91-2.mol

Synonyms:(2,6-di-tert-butylphenyl)hydrogenphenylboronate

Chemical Property of (2,6-di-tert-butylphenyl)hydrogenphenylboronate

Chemical Property:

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Technology Process of (2,6-di-tert-butylphenyl)hydrogenphenylboronate

There total 1 articles about (2,6-di-tert-butylphenyl)hydrogenphenylboronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,6-di-tert-butylphenol (128-39-2) + phenylborondichloride (873-51-8) → (2,6-di-tert-butylphenyl)hydrogenphenylboronate (1037069-91-2)

Guidance literature:

With n-butyllithium; In hexane; toluene; byproducts: LiCl; n-C4H9Li in hexane was added dropwise to a soln. of phenol-compound in toluene in N2 atm., the mixt. was heated at 100°C overnight, cooled to room temp., Cl2BC6H5 was added, heated for 18 h; ppt. was dissolved washing with water, dried over MgSO4, the solvent wasremoved in vac.;

DOI:10.1021/ic800204q

upstream raw materials:

2,6-di-tert-butylphenol

phenylborondichloride