Technology Process of C15H20O3
There total 9 articles about C15H20O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine-SO3 complex; TEA; dimethyl sulfoxide;
In
dichloromethane;
at 20 ℃;
for 0.5h;
DOI:10.1016/j.tet.2007.07.005
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 3.59 g / imidazole / CH2Cl2 / 1 h / 20 °C
2: 98 percent / TEA / CH2Cl2 / 0 - 20 °C
3: 84 percent / CSA; methanol / 2 h / 20 °C
4: 80 percent / sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C
5: 91 percent / sodium hexamethyldisilazide / dimethylformamide; tetrahydrofuran / 0 - 20 °C
6: 92 percent / TBAF / tetrahydrofuran / 12 h / 20 °C
7: 92 percent / SO3*pyridine; TEA; DMSO / CH2Cl2 / 0.5 h / 20 °C
With
1H-imidazole; methanol; pyridine-SO3 complex; TEA; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; dimethyl sulfoxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
4: Williamson ether synthesis;
DOI:10.1016/j.tet.2007.07.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / sodium hexamethyldisilazide / dimethylformamide; tetrahydrofuran / 0 - 20 °C
2: 92 percent / TBAF / tetrahydrofuran / 12 h / 20 °C
3: 92 percent / SO3*pyridine; TEA; DMSO / CH2Cl2 / 0.5 h / 20 °C
With
pyridine-SO3 complex; TEA; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; dimethyl sulfoxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.07.005
