Technology Process of C15H11NO2S
There total 4 articles about C15H11NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H19NO4S;
With
sodium hydroxide;
In
1,2-dimethoxyethane; water;
at 60 ℃;
for 2h;
With
hydrogenchloride;
In
1,2-dimethoxyethane; water;
at 60 ℃;
for 2h;
Further stages;
DOI:10.1016/j.bmc.2012.04.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / 1,3-dimethyl-2-imidazolidinone; mineral oil / 0.33 h / 0 - 20 °C / Inert atmosphere
1.2: 4 h / 120 °C / Inert atmosphere
2.1: sodium hydroxide / 1,2-dimethoxyethane; water / 2 h / 60 °C
2.2: 2 h / 60 °C
With
sodium hydride; sodium hydroxide;
In
1,3-dimethyl-2-imidazolidinone; 1,2-dimethoxyethane; water; mineral oil;
DOI:10.1016/j.bmc.2012.04.008
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: polyphosphoric acid / 5 h / 200 °C / Inert atmosphere
2.1: sodium hydride / 1,3-dimethyl-2-imidazolidinone; mineral oil / 0.33 h / 0 - 20 °C / Inert atmosphere
2.2: 4 h / 120 °C / Inert atmosphere
3.1: sodium hydroxide / 1,2-dimethoxyethane; water / 2 h / 60 °C
3.2: 2 h / 60 °C
With
sodium hydride; sodium hydroxide;
In
1,3-dimethyl-2-imidazolidinone; 1,2-dimethoxyethane; water; mineral oil;
DOI:10.1016/j.bmc.2012.04.008