(3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine

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Chemical Name:(3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine
CAS No.:1049705-32-9
Molecular Formula:C₂₅H₂₅NO₄
Molecular Weight:403.478
Hs Code.:

Synonyms:(3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine

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Chemical Property of (3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine

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Technology Process of (3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine

There total 1 articles about (3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1049705-30-7
(3R,7R,8aS)-6-(benzyloxycarbonyl)-8a-(3-butenyl)-5-oxo-3-phenyl-7-vinyl-2,3,6,7,8,8a-hexahydro-5H-oxazolo[3,2-a]pyridine

: 1049705-32-9
(3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jo801172b

Reference yield: 83.0%

: 1049705-32-9
(3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine

: 1049705-34-1
(3R,7S,12S)-7,12-methano-5-oxo-3-phenyl-2,3,5,6,7,8,9,10,11,12-decahydrooxazolo[3,2-a]azonine

Guidance literature:: (3R,7R,12S)-6-(benzyloxycarbonyl)-3-phenyl-7,12-methano-5-oxo-2,3,5,6,7,10,11,12-octahydrooxazolo[3,2-a]azonine; With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 48h; atmospheric pressure;

In toluene; for 20h; Further stages.; Heating;
DOI:10.1021/jo801172b